Analyses and Tests

AnalysesEQUIPMENTDESCRIPTIONVALUECONTACTSTANDARDNOTES
GPCLC-20AD ShimadzuSolved molecules separation on the basis of sizeR$ 850 / sample.LCP
ricardo.machado@ufsc.br
+55 (48) 3721 2690
Samples must be soluble in THF.
Scanning electron microscopy (Topographic images, elemental mapping)SEM (TM 3030/ 2014)R$ 200 /hCERMAT
+55 (48) 3721 7223
Sample preparation not included.
Scanning electron microscopyJEOL JSM-6390LV Scanning Electron MicroscopeTungsten filament, accelerating volttages of 0.5 - 30kV, magnification of 25 – 300000 times, High voltage resolution: 3 nm; low voltage resolution: 4nm.R$ 250 /hLCME
+55 (48) 3721-8727
+55 (48) 3721-2276
Sample’s diameter shall not be larger than 15 cm. Low vacuum mode included.
Scanning electron microscopyJEOL JSM-6701F Scanning Electron MicroscopeCold cathode: Field emission (FESEM), High resolution: 1nm(30kV)- 2.2n (1.2kV), Accelerating volttage: 0.5 to 30kV, Magnification 25 to 650000 times.R$ 400 /hLCME
+55 (48) 3721-8727
+55 (48) 3721-2276
Transmission electron microscopyJEM – 1011 TEMMaximum volttage acceleration: 100 kV, Resolution 0,45 nm, Line image resolution: 0,20 nm, Magnification range: 800 to 600.000 times, Goniometer inclination stage: ±20ºR$ 250 /hLCME
+55 (48) 3721-8727
+55 (48) 3721-2276
Transmission electron microscopyJEM – 2100 TEMMaximun accelerating valttage: 200 kV, Magnification: 2000 to 1.200.000 times, Point image resolution: 0,23 nm, Line image resolution: 0,14 nm, Goniometer inclination stage: ±30ºR$ 600 /hLCME
+55 (48) 3721-8727
+55 (48) 3721-2276
Confocal

microscopy
Leica DMI6000 B MicroscopeConfocal Scanner TCS SP5 attached, Diode laser on UV line 405 nm, Ar Laser in: 458, 476, 488, 496, 514 nm. He-Ne laser in: 543, 594 e 633 nmR$ 300 /hLCME
+55 (48) 3721-8727
+55 (48) 3721-2276
Laser diffraction particle size analyserMastersizer 2000 HydroParticle size range 6 nm to 2000 µm, Dispersion in liquid environmentR$ 200 /hFarmaceutical Technology and Cosmetology Laboratory

lemos.senna@ufsc.br, carolmmoreira@hotmail.com,

+55 48 3721 5067
Dermal permeation and liberation of nanoencapsulated compoundsDist e USP 4 Erweka Dermal permeation evaluation. Farmaceutical Technology and Cosmetology Laboratory

lemos.senna@ufsc.br, carolmmoreira@hotmail.com,

+55 48 3721 5067
Costs are discussed with the company.
Size measurement by Dynamic Light ScatteringZetasizer Nano Malvern ZS/2011Particle size range: 0.0003 to 10 µm, Dispersion in liquid environmentR$ 100 / sampleLaCBio
lacbio@contato.ufsc.br,

+55 48 3721-6570
ASTM B821, ASTM B822DLS cuvettes are only given for outside users.
Size measurement by Dynamic Light ScatteringZetasizer Nano Malvern ZSParticle size range: 0.0003 to 10 µm, Dispersion in liquid environmentR$ 100 / sample
GEIMM
+55 48 37212212
Size measurement by Dynamic Light ScatteringZetasizer Nano Malvern ZSParticle size range: 0.0003 to 10 µm, Dispersion in liquid environmentR$ 100 / sampleLINDEN-metro
+55 (48) 3721 3633
ISO 22412:2017
Size measurement by Dynamic Light ScatteringNanoflex MICROTRACParticle Size range: 0.8 nm to 6.5 µm, Dispersion in liquid environmentR$ 100 / hLINDEN-metro
+55 (48) 3721 3633
ISO 22412:2017
Zeta PotentialStabino ParticleMetrixZeta Potential evaluation (1 point) and Isoelectric point determination (Titration ZP x pH).R$ 100 / hLINDEN-metro
+55 (48) 3721 3633
Zeta PotentialZetasizer Nano Malvern ZSZeta Potential evaluation (1 point) and Isoelectric point determination (Titration ZP x pH).R$ 100 / hLINDEN-metro
+55 (48) 3721 3633
ISO 13099-2:2012
Qualitative and Quantitative Phase Analysis of Polycrystalline MaterialsMiniFlex600 DRX RigakuScanning range: 3 to 140°.
Powders samples.
R$ 150 / h / sampleLINDEN-metro
+55 (48) 3721 3633
Particle and droplet velocity distributions for creaming and sedimentation phenomenaLUMISIZER (L.U.M GmbH / 2014)Particle size range: 10 nm to 10000 µmR$ 100 / sampleLINDEN-metro
+55 (48) 3721 3633
ANALYSESEQUIPMENTDESCRIPTIONVALUECONTACTSTANDARDNOTES
Atomic

Absorption Spectrometry
AA – 6300 ShimadzuMetal identification and quantification. Available lamps: Al, Sb, As, Cd, Ca, Pb, Co, Cu, Cr, Fe, Mg, Mn, Mo, Ni, K, Ag, Na, ZnR$ 80,00Prof. Antônio Augusto Ulson de Souza*

+55 48 3721 5231
Contact angle250-F1 Ramé-HartMeasurement of contact angle between solid and liquid surfaces.R$ 100 / sampleLCP
ricardo.machado@ufsc.br
Enzymatic activityTermostatized

Bath,Dist Spectrophotometer UV mini 1240 Shimadzu
Measuremente of enzymatic activity in a reaction.R$ 200Prof. Antônio Augusto Ulson de Souza*

+55 48 3721 5231
Gass chromatographyCG – 2010 ShimadzuGaseous and volatile compounds separation.R$ 150 / sampleLCP
ricardo.machado@ufsc.br
ColorimeterCM – 3600 A Konica MinoltaQuantification of color variation in tissues, papers and liquid samples. Wavelength range: 360 to 740 nmR$ 20,00Prof. Antônio Augusto Ulson de Souza*

+55 48 3721 5231
ConductivityQ405. PMeasurement of conductivityR$ 20 / sampleLCP
ricardo.machado@ufsc.br
Gass chromatographyCG – 17A Shimadzu Auto injetor AOC 5000Quantifications of known compounds according to reference standard.R$ 150,00Prof. Antônio Augusto Ulson de Souza*

+55 48 3721 5231
Gas chromatography – massCG 3900 acoplado ao Saturn 2100T – Marca VarianIdentification and quantification of unknown compoundsR$ 250,00Prof. Antônio Augusto Ulson de Souza*

+55 48 3721 5231
BODVELP ScientificaBiochemical oxygen demandR$ 150,00Prof. Antônio Augusto Ulson de Souza*

+55 48 3721 5231
DSC - Differential scanning calorimetrySTA 449-F3 Jupiter (2012)Heat flow into or out of a sample is measured as a function of temperature.R$ 120 /sample.LCP
ricardo.machado@ufsc.br
CODTR 320 SpectroquantChemical oxygen demand.R$ 100,00Prof. Antônio Augusto Ulson de Souza*
+55 48 3721 5231
FTIRIR Prestige 21 Shimadzu (2012)Organic and inorganic componds characterization, according to functional groups bands.R$ 120 / sampleLCP
ricardo.machado@ufsc.br
Samples must be powders or solid that can be triturated.
Muffle furnaceEDG 3P-S EDG EquipamentosSolid and volatile compounds determination.R$ 50 / hProf. Antônio Augusto Ulson de Souza*
+55 48 3721 5231
pHAN 2000PH measurmentR$ 20 / sample.LCP
ricardo.machado@ufsc.br
Critical point.Leica EM CPD030R$ 100LCME
MEV - Preparation with coatingLeica EM SCD 50030 nm coatingR$ 100LCME
TEM - Preparation on GridR$ 100LCME
TEM – Preparation

Plan View
R$ 800LCME
TEM – Preparation

Cross Section
R$ 1000LCME
Ash contentMuffle furnace EDG 3P – S EDG EquipamentosDetermination of inorganic compounds

content
R$ 50,00Prof. Antônio Augusto Ulson de Souza*
+55 48 3721 5231
NBR 8112 (1986)
Moisture contentHeating chamber TE – 393/1 TECNALDetermination of water contentR$ 50,00Prof. Antônio Augusto Ulson de Souza*
+55 48 3721 5231
NBR 8112 (1986)
Moisture contentHeating chamber TE – 393/1 TECNALDetermination of water contentR$ 50,00Prof. Antônio Augusto Ulson de Souza*
+55 48 3721 5231
NBR 8112 (1986)
TOCTOC – V CPH ShimadzuCarbon content quantificationR$ 150,00Prof. Antônio Augusto Ulson de Souza*
+55 48 3721 5231
UltracentrifugationBeckman Coulter – OptimaTM MAX-XP UltracentrifugeParticle separation.R$ 200/ hlemos.senna@ufsc.br, carolmmoreira@hotmail.com

+55 48 3721 5067
UltramicrotomyLeica EMUC7 Power Tome XLGlass or diamond razors.R$ 800LCME
UV-visible spectrophotometryShimadzu UV spectrophotometerUV-visible spectrophotometryR$ 500 / samplelemos.senna@ufsc.br, carolmmoreira@hotmail.com,

+55 48 3721 5067
Compond determination
UV-visible spectrophotometryUV mini 1240 ShimadzuWavelength range: 190 to 1100nm.R$ 50 / sampleProf. Antônio Augusto Ulson de Souza*
+55 48 3721 5231
UV-visible spectrophotometryU-1900 Hitachi (2008)visible light, near-ultravioletR$ 100 / sampleLCP
ricardo.machado@ufsc.br